Structure
By Guan-Qun Han and Yan-Ru Liu and Wen-Hui Hu and Bin Dong and Xiao Li and Xiao Shang and Yong-Ming Chai and Yun-Qi Liu and Chen-Guang Liu
	
			
	
				Published in International Journal of Hydrogen Energy
	
	
	
				2016
	
			
Abstract
Nanostructured plate-like island molybdenum sulfides (MoSx) film has been synthesized successfully through a facile one-step electrodeposition method from the mixture solution of N, N-dimethyl-formamide (DMF) and H2O. The effect of different ratio of \DMF\ to \H2O\ on the MoSx film has been investigated. Scanning electron microscopy (SEM) shows that when the ratio of \DMF\ to \H2O\ is 1:20, the as-prepared MoSx film exhibits maximum island structures, exposing most edges and rims. The electrochemical measurements confirm that MoSx film deposited in the mixed solution of VDMF: VH2O

