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// Electrochemical Cells line

Dr. Bob's Cell

Small-volume electrochemical cell kit
Cited in the literature See research citations →

The smallest cell in the range, working between 1 and 30 mL across five multi-purpose ports, jacketed or unjacketed.

What it does
  • Smallest cell in the range — 1-30 mL, down to 1-2 mL in the pear-shaped flask
  • Five multi-purpose ports, with a central Ace-Thread for the working electrode
  • Takes any of Gamry's working electrodes
  • Jacketed and non-jacketed versions
  • Suits enzyme and catalysis studies, sensor development, battery mechanism work and redox potentials of inorganic complexes
For applications including
// Research citations

Cited in the literature

Independent research citations for this instrument are provided by Bioz and appear here once the widget loads.

Citation data provided by Bioz.
// Overview

The Dr. Bob's Cell™ is our smallest electrochemical cell kit, with operational volumes of 1-30 mL.  Enzyme and catalysis studies, development of electrochemical sensors, basic research into battery mechanisms, and determination of redox potentials of inorganic complexes represent a few of its many applications.  Designed for flexibility and convenience, this cell kit can hold any of Gamry’s available working electrodes.  It's available in both a non-jacketed model and a jacketed version for temperature control.

Product Details

Overview

Dr. Bob's Cell utilizes a pear-shaped flask which permits handling low volumes (down to 1-2 mL*). It is equipped with 5 multi-purpose ports. In the normal cell configuration, these ports are used as follows:

  • One central Ace-Thread port for a Working Electrode (ordered separately)
  • One Ace-Thread port for a Luggin capillary/bridge tube for use with Gamry’s SCE, Ag/AgCl, and Hg/Hg2SO4 reference electrodes (electrodes ordered separately)
  • One Ace-Thread port for a glass frit isolated platinum wire counter electrode (a wire is supplied)
  • One 14/20 ground glass port for inert gas purging/blanketing (an adapter is supplied)
  • One 14/20 ground glass port usable for temperature sensing, reagent addition, gas venting, etc.

The Ace-Threads allow for vertical adjustment to accommodate a wide range of sample volumes. Because the Dr. Bob’s Cell uses standard joints and fittings, you can easily customize it for specific applications. The bubbler has one position for deaeration and another for blanketing. We include a 2 x 6 mm PTFE magnetic spin bar with all kits. A jacketed model is available for temperature control. The non-jacketed model includes a stand.

Working Electrodes are available in Platinum, Carbon (Glassy or Fiber), and Gold. They may be obtained in either a macro version with a 3 mm diameter or as a microelectrode with a 10 micron diameter. The macro electrodes have a Kel-F body and all electrodes are tested prior to shipment by running a cyclic voltammogram on a ferricyanide sample.

*Note that for working in volumes below 5 mL some modifications may be necessary to the standard setup; e.g. removal of the counter bridge tube.

Accessories

Parts available for the Dr. Bob's Cell include:

// Specifications

The complete technical detail

Dimensions
Working VolumeBetween 1 mL and 30 mL
SizeApproximately 10 cm diameter by 30 cm high(including electrodes)
Working Electrode Port
Type#7 Ace-Thred
Electrode DiameterSupports 6.5 mm to 7.5 mm diameter electrode bodies
Electrode LengthFor work with small volumes, length must be at least 11 cm
Macro ElectrodesGlassy carbon, gold, and platinum (3 mm diameter)
Micro Electrodes10 μm gold and platinum electrodes and 11 μm carbon fiber
Reference Electrode Port
Type#7 Ace-Thred - includes a standard reference electrode bridge tube
Reference Electrode Diameter9 - 11.5 mm (when used with the bridge tube)
Bridge tube termination in electrolyteUnfired Porous Glass disk, 3.5 mm diameter
Counter Electrode Port
Type#7 Ace-Thred – comes equipped with fritted glass isolation tube
Counter Electrode0.41 mm diameter platinum wire, approx 150 mm long
Gas Flow Port
Type14/20 - equipped with three-way gas flow adapter (purge, blanket, vent)
Spare Port
Type14/20 - supplied with several polyethylene stoppers
Chemical Compatibility
Wetted MaterialsPyrex®, PTFE, unfired Porous Glass, ACE FETFE, Platinum, Polyethylene
Non-Wetted MaterialsAbove, plus nylon

Product video

Dr. Bob's Electrochemical Cell Demo
// Resources

Documentation