“Protective shield opens on the side which can be a bit awkward - I do wish it were front opening. That said, this instrument is great! The software is easy to use and the instructions provided to set up the instrument were easily understood. I am pleased with the quality of the tool, the analytical software, and the insights gained from the data. I appreciate the versatility of the system and the option to rotate at low to high RPM. ”
Rotating Electrode
- Research-grade rotator
- Ability to use rotating ring-disk, disk and cylinder electrodes
- Corrosion, Catalyst Development, Fuel Cell Research Applications
Cited in the literature
Independent research citations for this instrument are provided by Bioz and appear here once the widget loads.
The RxE 10kTM Rotating Electrode (Part #992-00146) is a research-grade rotator and features the ability to use rotating ring-disk and cylinder electrodes. It can be used as the working electrode in any electrochemical cell with any Gamry potentiostat.
The RxE is digital (USB) or analog controlled. Rotation rates are 50-10500 rpm. Our one-piece shaft design actually allows us to rotate at those speeds. The RxE accuracy over this rotation rate range is +/- 1rpm.
- Includes:
• Rotator
• Baseplate with adjustable height stand
• Motor Control Unit and control cable
• Power Supply
• USB Cable
Does not include shaft
Product Details
Overview
The RxE 10k Rotating Electrode is a research-grade rotator and features the ability to use rotating ring-disk, disk and, cylinder electrodes. The rotation rate is adjustable from 50 – 10500 rpm (revolutions per minute). The Controller has a Liquid Crystal Display (LCD) which indicates the rotation rate and is controlled by a rotation rate knob. Alternatively, the rotation rate may be controlled by your Gamry Interface or Reference family instrument. The electrode assembly of the rotator has a versatile design that allows for the use of diverse electrode types. Different shaft and electrode tips can be selected depending on your desired use. Different shafts are used for disk and cylinder or ring–disk experiments.
Applications
- Corrosion
- Catalyst Development
- Fuel Cell Research
- Controlling Mass Transport of Reactants to Electrode Surface
Rotating ring-disk electrodes are used where products generated at the disk electrode are monitored at the ring electrode. A bipotentiostat is required for these experiments and Gamry can supply an instrument using two standard Gamry Potentiostats collecting data synchronously when connected to the same computer. A number of ring-disk electrodes are available including platinum-platinum, gold-gold and glassy carbon-glassy carbon.
Rotating disk experiments are performed where defined mass transport to the sample electrode is desired. An example of this type of experiment would be catalyst evaluation.
Rotating cylinder experiments are important in the oil industry to simulate the corrosion environment inside a pipeline, thus avoiding the need to assemble expensive flow loop setups. The rotator is an ideal tool because flow conditions at the rotating cylinder are generally turbulent even at low rotation rates. Cylinders can be made from a variety of different metals to evaluate their performance including 1018 carbon steel, 316 stainless steel and 430 stainless steel. Users can machine cylinder samples using their actual material.
The electrodes for the rotator are sold separately and include a wide selection of standard materials such as gold, platinum, glassy carbon, carbon steel, stainless steel, etc. Custom materials are available on request.
Accessories
Available at our on-line store
RDEDimensions:
|
|
| GC | |
| 976-00002 | Pt |
| 976-00003 | Au |
| 990-00538 | RDE/RCE Shaft |
RCEDimensions:
|
|
| 977-00010 | Body Only |
| 977-00102 | 1018CS |
| 977-00103 | 316SS |
| 977-00104 | 430SS |
| 990-00538 | RDE/RCE Shaft |
RRDEDimensions:
|
|
| 978-00001 | Pt-GC (R-D) |
| 978-00002 | GC-GC |
| 978-00003 | Pt-Pt |
| 978-00004 | Au-Au |
| 990-00539 | RRDE Shaft |
The complete technical detail
| Power | 100 - 240 VAC, +/-10%; 50/60 Hz; 2A |
|---|
| Shipping Weight | 60 pounds (25 kg) |
|---|---|
| Shipping Dimensions | 24.0 x 20.0 x 24.0 in (61 x 51 x 61 cm) |
| Control Unit | 11.4 x 10.1 x 5.75 in (29 x 26 x 15 cm) |
|---|---|
| Rotator Enclosure: | 18.8 x 15.5 x 21.0 in (48 x 40 x 54 cm) |
| Motor Power | 147 W rated power |
|---|---|
| Supply Voltage | 48 VDC |
| Motor Type | Brushless DC (BLDC) motor |
| Motor Protection | 2 Amp thermal-type circuit breaker current limited power supplies |
| Max. Continuous Torque | 30 millinewton-meters |
| Rate Control | closed loop servo-system temperature compensated tachometer mounted on motor shaft |
| Rate Display | 4 ½ digit display indicates rotation rate (RPM) |
| Rate Accuracy | +/- 1 rpm for 50-10500 rpm |
| Front Panel | Analog and Digital Control |
|---|
| Max distance between baseplate and mounted electrode tip | 263 cm (RDE); 258 cm (RCE); 261 cm (RRDE) |
|---|
Specifications are drawn from this product page and are pending datasheet verification — see SPEC-VERIFICATION.md.